MIL-STD-867C
TABLE III
(Limited Access or Swab Etch Technique)
STEP |
PROCESS |
SOLUTION |
TIME |
TEMPERATURE |
REMARKS |
1. |
Solvent clean |
Cleaner A-A- 59281 or ASTM- 0329 |
As necessary |
Ambient |
Wipe surface with commercial cheese cloth saturated with solvent. Wipe dry with cheese cloth. |
2. |
Nitric acid etch |
Nitric acid (A-A-59105) 4% to 10% (by volume) in alcohol (27CFR 21.35, Formula 3-A) |
Until a black smutty etch is produced. |
Ambient |
Swab the surface with commercial grade cheese cloth saturated with Nitric solution. The more concentrate solution reduces time. |
3. |
Rinse |
Acetone (ASTM-0329) |
To remove nitric acid |
Ambient |
Rinse immediately |
4. |
Acid clean |
Hydrochloric acid (ASTM- E1146) 6% to 10% (by volume) in water |
To remove black smut. |
Ambient |
Swab with commercial cheese cloth saturated with HCL solution. |
5. |
Rinse |
Clean water |
To remove HCL |
Ambient |
Swab with commercial cheese cloth saturated with water. |
6. |
Neutralize |
Any alkali solution with pH of 10 minimum |
To neutralize HCL |
Ambient |
Swab with commercial cheese cloth saturated with alkali solution. |
7. |
Rinse |
Clean water |
To remove caustic |
Ambient |
Swab with commercial cheese cloth saturated with water. |
8. |
Rinse |
Alcohol |
To remove water |
Ambient |
Swab with commercial cheese cloth saturated with alcohol and wipe dry. |
9. |
Inspect and evaluate per appropriate criteria. |
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*10. |
Oil |
Rust preventative MIL-PRF-16173 |
Swab only |
Ambient |
To prevent corrosion. |
Steps 1 thru 9 shall be completed without interruption. |
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* Apply the oil after the required embrittlement relief bake. This step may be omitted if the facility can show evidence that corrosion during the queue between process steps is not an issue. This could be the case in a low humidity environment. |
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